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. Author manuscript; available in PMC: 2010 Apr 15.

Published in final edited form as: J Am Chem Soc. 2009 Apr 15;131(14):5313–5320. doi: 10.1021/ja900067c

Table 1.

Selected X-ray data for 2, 17, 3, and 20.^a

	2^b	17	3^c	20

Bond Length (Å)
Ru-C(1)	1.980	1.968	1.962	1.964
RuC(25)	1.824	1.840	1.823	1.835
Ru-O	2.262	2.255	2.244	2.261

Bond Angles (deg)
C(3)-N(2)-C(16)	118.22	122.60	119.91	119.82
C(2)-N(1)-C(7)	118.32	123.82	120.69	120.26
C(1)-Ru-C(25)	101.42	103.08	102.48	103.14
C(1)-Ru-Cl(2)	156.42	161.26	159.49	160.80

^a

For a complete list of bond lengths and angles for 17 and 20, refer to the SI.

^b

See ref 4.

^c

See ref 5c.