Table 3.
entry | ynamides | R1 = | amidines | NR2 = | isolated yield [%] |
---|---|---|---|---|---|
1 | 29a | TBDPS | 30a | pyrrolidinyl | 95 |
2 | 29b | TBS | 30b | pyrrolidinyl | 94 |
3 | 29c | TES | 30c | pyrrolidinyl | 87 |
4 | 29d | (CH2)3OTBS | 30d | c-hex-NH | 41 |
5 | 29e | c-hex | 30e | pyrrolidinyl | 54 |
6 | 29e | c-hex | 30f | c-hex-NH | 69 |