Table 1. Data-collection statistics.
Space group | I222 or I212121 |
Unit-cell parameters (Å) | a = 48.6, b = 61.9, c = 79.6 |
No. of molecules in the unit cell | 4 |
VM (Å3 Da−1) | 2 |
Solvent content (%) | 39 |
Resolution range (Å) | 43.2–2.7 (2.8–2.7) |
Total No. of measured reflections | 17521 |
No. of unique reflections | 3285 |
Completeness (%) | 98.7 (98.9) |
Rmerge† (%) | 10.9 (49.7) |
Rr.i.m.† (%) | 11.8 (59.1) |
Rp.i.m.† (%) | 9.4 (34.2) |
Average I/σ(I) | 5.4 (2.0) |
R merge = , R r.i.m. = , R p.i.m. = (Weiss, 2001 ▶).