Skip to main content
. Author manuscript; available in PMC: 2010 Apr 15.
Published in final edited form as: J Am Chem Soc. 2009 Apr 15;131(14):5344–5349. doi: 10.1021/ja8100775

Figure 2.

Figure 2

Fully protonated denatured 15N Ala Galectin-3 (a) and partially deuterated 15N Ala Galectin-3 (b–f) The HSQC spectra are acquired in a 600 MHz spectrometer at 5°C in ~ 8 M protonated urea pH 2.4 (a) and pD 3.1 (b–f) respectively. The small offsets apparent in the proton dimension between the fully protonated sample (a) and the exchanging spectra (b-f) may arise differences in lock frequencies for HDO (10% D2O) vs D2O (~100% D2O).