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. Author manuscript; available in PMC: 2010 Feb 17.
Published in final edited form as: Biochemistry. 2009 Feb 17;48(6):1162–1172. doi: 10.1021/bi802211k

Table 1.

1H and 13C NMR assignments (ppm from TMS) and coupling constants (J, Hz) of the GalN residue in undecaprenyl phosphate-GalN

GalN H-1
(J 1,2)		 H-2
(J 2,3)		 H-3
(J 3,4)		 H-4
(J 4,5)		 H-5
(J 4,5)		 H-6a
(J 5,6a)
(J 6a,6b)		 H-6b
(J5,6a)
(J6a,6b)
δH 5.065
(8.2)		 3.217 3.77
(3.1)		 3.907 3.671 3.789
(6.7)
 3.725
(5.3)
C-1 C-2 C-3 C-4 C-5 C-6
δC 96.12 55.26 70.46 68.66 77.08 61.98

1H chemical shifts (ppm from TMS) are from 1D 1H spectra with a digital resolution of 0.2 Hz per point. Coupling constants (JH,H, Hz) were measured from the 31P-decoupled 1H NMR spectra. 13C chemical shifts (ppm from TMS) were estimated from the 2D HMQC spectra.