Table 1.
Alkene | Temperature (°C) | Residence Time (min)b | Conversion (%) | Yield (%)b |
70 | 2.6 (2) | 100.0 | 99.1 (6.7)c | |
70 70 |
2.6 5.2 (33) |
57.2 100.0 |
– 99.2 (3.6) |
|
70 | 2.6 (40) | 100.0 | 97.6 (5.9) | |
70 70 |
2.6 5.2 |
31.9 100.0 |
– 99.5 (5.9) |
|
70 70 |
2.6 5.2 |
32.1 100.0 |
– 99.1 (5.9) |
The number in parentheses represents athe reaction time required under batch conditions (h) [21], bthe isolated yield obtained after continuous operation of the reactor for 24 h and cthe throughput (mg h−1) using the optimised conditions.