Table 3.
| |||
---|---|---|---|
Entry | R | Product | % Yield[b] |
1 | OMe | 2 | 95 |
2 | OEt | 3 | 92 |
3 | OH | 4 | 94 |
4 | Me | 5 | 79 |
5 | NH2 | 6 | 81 |
Reaction conditions: 1 (0.12 mmol), Pd2(dba)3·CHCl3 (2mol-%), methyl acrylate (0.36 mmol), Bu4NCl (0.12 mmol) in DMF at 110 °C for 14 h.
Isolated yields.