Table 1.
Correlation features observed in the gZ-HYSCORE spectra of the LS form of Cyt c6
| Frequency (MHz)∗ | 14N-Hem† | 14N-His† | 1H† | Label‡ |
|---|---|---|---|---|
| Single nuclear correlation features | ||||
| 11.6, 9.0 | ++ | LZ1 | ||
| 6.9, −4.1 | ++ | LZ2 | ||
| 6.9, −2.7 | + | |||
| 6.9, −1.4 | + | |||
| 6.2, −3.4 | ++ | LZ3 | ||
| 6.2, −0.6 | + | |||
| 4.2, 0.6 | + | |||
| 4.1, −2.9 | + | |||
| 4.0, −1.4 | + | |||
| 2.9, −2.7 | + | |||
| 2.9, 1.4 | + | |||
| 2.9, −0.6 | + | + | ||
| 2.8, −2.0 | + | |||
| 2.0, −0.6 | + | |||
| Combination features | ||||
| 17.0, −4.1 | + | + | ||
| 16.4, −3.4 | + | + | ||
| 13.8, −8.2 | + | LZ4 | ||
| 13.1, −7.5 | + | + | LZ5 | |
| 12.7, −2.7 | + | + | ||
| 10.9, −4.2 | + | |||
| 8.2, −6.9 | + | |||
| 7.4, −6.3 | + | + | ||
| 4.1, −0.4 | + | + | ||
The accuracy in frequency is ±0.2 MHz.
The minus sign in the second frequency value indicates that the feature is detected in mainly the second, (+, −), quadrant of the HYSCORE frequency spectra.
Double plus signs denote signals assigned to 14N dq-dq correlations and to 1H correlations. Other correlations are indicated by single plus signs.
For some signals, a label was given to identify them in figures and text.