Table 3.
Correlations observed in the gZ-HYSCORE spectra of the HALS form of Cyt c6
| Frequency (MHz)∗ | 14N-Hem† | 14N-His† | 1H† | Label‡ |
|---|---|---|---|---|
| Single nuclear correlation features | ||||
| 11.0, 7.7 | ++ | HZ1 | ||
| 6.6, −4.2 | ++ | HZ2 | ||
| 5.8, −3.4 | ++ | HZ3 | ||
| 3.9, −2.8 | + | |||
| 3.9, −1.4 | + | |||
| 3.7, −3.4 | + | |||
| 3.7, −0.9 | + | |||
| 2.8, −2.7 | + | |||
| 2.8, −2.1 | + | |||
| 2.1, −0.9 | + | |||
| Combination features | ||||
| 15.2, 1.1 | + | + | HZ4 | |
| 12.8, −8.2 | + | |||
| 12.4, −7.6 | + | + | ||
| 10.5, −4.2 | + | |||
The accuracy in frequency is ±0.2 MHz.
The minus sign in the second frequency value indicates that the feature is detected in mainly the second, (+, −), quadrant of the HYSCORE frequency spectra.
Double plus signs denote signals assigned to 14N dq-dq correlations and to 1H correlations. Other correlations are indicated by single plus signs.
For some signals, a label was given to identify them in figures and text.