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. Author manuscript; available in PMC: 2009 Jul 27.
Published in final edited form as: Chem Commun (Camb). 2008 Aug 27;(1):20–33. doi: 10.1039/b809676g

Table 7.

Cross coupling vs. Heck reaction with 13

graphic file with name nihms92008t7.jpg
n-Bu4X (equiv.) Base (equiv.) Pd source Solvent 14 : 2
n-Bu4NOAc (2.5) — Pd(OAc)2 DMF 99 : 1
n-Bu4NCl (2.5) KOAc (2.5) Pd(OAc)2 DMF 90 : 10
n-Bu4NCl (1) TBAF (1.3) Pd(dba)2 Toluene 12 : 84
n-Bu4NCl (2) KF (3) Pd(dba)2 Toluene 8 : 92