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. Author manuscript; available in PMC: 2009 Jul 29.
Published in final edited form as: J Org Chem. 2008 Aug 2;73(17):6480–6488. doi: 10.1021/jo8008534

FIGURE 4.

FIGURE 4

1H,1H TOCSY spectrum (CDCl3, 298 K) showing 3JH,H coupling between the DABCO methylene protons and the proton shared by the base and the acid of host H2a. This coupling reveals that the acid proton has been at least partially transferred to a nitrogen of DABCO.