Table 1.
Data collection and refinement statistics
| Data collection | MOA in complex with Galα (1,3)[Fucα (1,2)]Gal |
|---|---|
| Space group | P3 |
| Cell parameters | |
| a, b, c (Å) | 121.3, 121.3, 100.0 |
| α β γ (°) | 90, 90, 120 |
| Wavelength (Å) | 0.934 |
| Resolution (Å) | 47-1.8 (1.9-1.8) |
| Rmerge (%) | 10.9 (47.1) |
| I / σI | 12.5 (3.3) |
| Completeness (%) | 99.2 (98.2) |
| Multiplicity | 8.8 (5.1) |
| Refinement | |
| Resolution (Å) | 30-1.8 |
| No. unique reflections | 143810 |
| Rwork / Rfree (%) | 16.4/18.9 |
| R.m.s deviations from ideal values30 | |
| Bond lengths (Å) | 0.012 |
| Bond angles (Å) | 1.41 |
| Average/Wilson B-factor (Å2) | 11.8/13.5 |
| Real space correlation coefficient | 0.95 |
| Ramachandran outliers (%)1 | 2.5 |
| PDBid | 3EF2 |
Values for the highest resolution shell are shown in parenthesis.
1
Ramachandran analysis performed as described31.