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. Author manuscript; available in PMC: 2009 Aug 6.
Published in final edited form as: J Chromatogr A. 2006 Sep 1;1133(1-2):248–253. doi: 10.1016/j.chroma.2006.08.042

Fig. 5.

Fig. 5

One-step preparative RP-HPLC purification of trace levels of TM 1–99. Conditions: same as Fig. 4. Sample volume: 5 ml (60 ml of lysate had been freeze-dried and redissolved in 5 ml of 0.1% aq. TFA). The top panel shows the analytical RP-HPLC profile of the crude sample mixture. P denotes desired product which represents <0.1% of total contents of crude sample.