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. 2009 Jul 6;191(17):5499–5509. doi: 10.1128/JB.00121-09

TABLE 7.

Chemical shift assignments of WH8102 polysaccharide liberated from aqueous-phase LPS by hydrazinolysis

Residue Nucleus Chemical shift (ppm)
1 2 3 4 5 6
4-α-Glcp 1H 5.37 3.65 3.97 3.64 3.85 3.89/3.85
13C 100.6 72.4 74.2 78.5 72.4 61.6
α-Glcp 1H 5.37 3.62 3.73 3.45 3.71 3.87/3.79
13C 101.0 72.4 73.8 70.5 72.4 61.6
2,4-α-Glcp 1H 4.97 3.61 4.03 3.65 3.88 3.89/3.85
13C 99.6 79.9 74.2 78.5 72.4 61.6