Table 1.
Crystal form | EmrE-ethidium | EmrE-propidium | EmrE-dequalinium | |||
---|---|---|---|---|---|---|
Plane group symmetry | p2 | p2 | p2 | |||
Unit cell dimensions | ||||||
a (Å) | 74.57 ± 0.57 | 69.33 ± 0.51 | 70.05 ± 0.45 | |||
b (Å) | 89.93 ± 1.48 | 83.38 ± 0.46 | 83.92 ± 1.26 | |||
γ (deg.) | 106.69 ± 1.16 | 106.05 ± 0.54 | 105.75 ± 0.45 | |||
No. images | 12 | 7 | 5 | |||
Range of defocus (Å) | 4113_10488 | 6202_16069 | 5614_15612 | |||
No. unique reflections | 191 | 126 | 102 | |||
Total observations | 1694 | 805 | 615 | |||
Overall phase residual | 27.70 | 40.99 | 27.79 | |||
Temperature factor Bxy (Å) | 347 | 288 | 344 | |||
Resolution range (Å) | No. of unique reflections | Phase residuals | No. of unique reflections | Phase residuals | No. of unique reflections | Phase residuals |
∞–15.81 | 40 | 12.99 | 32 | 25.30 | 31 | 11.06 |
15.81–11.18 | 39 | 21.36 | 25 | 37.72 | 26 | 22.36 |
11.18–9.13 | 38 | 22.15 | 29 | 24.77 | 26 | 24.10 |
9.13–7.90 | 38 | 30.66 | 16 | 63.29 | 11 | 68.20 |
7.90–7.07 | 34 | 56.40 | 22 | 73.17 | 7 | 72.83 |
7.07–6.45 | 33 | 74.63 | 11 | 64.41 | 4 | 52.72 |
6.45–5.98 | 26 | 89.67 | 16 | 71.99 | 7 | 96.03 |