Table 3.
Entry | Substrate | Product | Yieldb |
---|---|---|---|
1 | 79% | ||
2 | 55% | ||
3 | 78% | ||
4 | 66% | ||
5 | 70% | ||
6 | 55% | ||
7 | 48% | ||
8 | 41% | ||
9 | 44% | ||
10 | 71% | ||
11 | 47% |
Reaction Conditions: 5 mol % Pd(OAc)2, 0-6 mol % bipy, 1.1-4 equiv PhI(OAc)2, 60-80 °C, 1-16 h.
Isolated yields (average of two runs).