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. Author manuscript; available in PMC: 2010 Jul 1.
Published in final edited form as: J Phys Chem C Nanomater Interfaces. 2009 Jul 1;113(31):13906–13917. doi: 10.1021/jp902736z

Figure 11.

Figure 11

1H MAS NMR spectra (9.4 T) obtained for nominally-dry Cu3(BTC)2: (a) initial spectrum; (b) – (d) after heating to 180 °C to drive off water and DMF; (e) – (f) after addition of 5 µL DMF; (g) after heating to 100 °C to re-adsorb DMF; and (h) after exposure to air to re-adsorb water. Spinning sidebands are marked by asterisks at the top of each stack.