Table IV.
NOE contact | Distance | NOE contact | Distance | ||||
---|---|---|---|---|---|---|---|
(Gal–Glc) | |||||||
Neu5Ac–Gal | rexpta | rMDb | rexpta | rMDb | |||
H3Ac | H3 | 2.8 ± 0.3 | 2.5 ± 0.8 | H1 | H4 | 2.3 ± 0.2 | 2.4 ± 0.2 |
H8 | H1 | 3.3 ± 0.3 | 6.2 ± 1.2 | H1 | H6A | 3.2 ± 0.3 | 3.6 ± 0.1d |
aData from (Siebert et al. 1992) for GM3 in DPC micelles and D2O, using a 10% estimate of the experimental error (Keepers and James 1984).
bStandard deviations reported.
cAxial hydrogen.
dSince the protons on C6 are indistinguishable, the average distance of both protons was used in the calculation.