Table 1.
Data collection and refinement statistics.
| All data (outer shell) | |
| Data Collection | |
| Space group | C2 |
| Cell dimensions | |
| a, b, c (Å) | 83.4, 143.8, 78.0 |
| α,β,γ (°) | 90.0, 121.6, 90.0 |
| Resolution (Å) | 37.96-2.00 (2.11-2.00) |
| Rmerge | 0.066 (0.315) |
| <I/σI> | 11.6 (3.3) |
| Completeness (%) | 95.3 (95.9) |
| Redundancy | 2.5 (2.5) |
| Refinement | |
| Resolution (Å) | 25.0-2.0 |
| No. of unique reflections | 47498 |
| Rcryst | 0.214 |
| Rfree | 0.259 |
| rms deviation from ideal values | |
| bond lengths (Å) | 0.023 |
| bond angles (°) | 2.171 |
| Number of atoms/au | 5498 |
| B factor (Å2) | |
| protein | |
| chain A | 28.5 |
| chain B | 28.5 |
| chain C | 21.3 |
| waters | 27.6 |
| Na+ ions | 22.0 |