Table 1.
All data (outer shell) | |
Data Collection | |
Space group | C2 |
Cell dimensions | |
a, b, c (Å) | 83.4, 143.8, 78.0 |
α,β,γ (°) | 90.0, 121.6, 90.0 |
Resolution (Å) | 37.96-2.00 (2.11-2.00) |
Rmerge | 0.066 (0.315) |
<I/σI> | 11.6 (3.3) |
Completeness (%) | 95.3 (95.9) |
Redundancy | 2.5 (2.5) |
Refinement | |
Resolution (Å) | 25.0-2.0 |
No. of unique reflections | 47498 |
Rcryst | 0.214 |
Rfree | 0.259 |
rms deviation from ideal values | |
bond lengths (Å) | 0.023 |
bond angles (°) | 2.171 |
Number of atoms/au | 5498 |
B factor (Å2) | |
protein | |
chain A | 28.5 |
chain B | 28.5 |
chain C | 21.3 |
waters | 27.6 |
Na+ ions | 22.0 |