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. Author manuscript; available in PMC: 2009 Sep 19.
Published in final edited form as: J Org Chem. 2008 Aug 27;73(18):7017–7027. doi: 10.1021/jo8015314

Table 1.

Neoglycoconjugate Formation with Protected Donors.

Neoglycosyl Donor Peptides Solvent Neoglycopeptide (Yield)
graphic file with name nihms86296t1.jpg graphic file with name nihms86296t2.jpg MeCN/
MeOH
(1:1)
graphic file with name nihms86296t3.jpg
graphic file with name nihms86296t4.jpg 15 MeCN/
MeOH
(1:1)
graphic file with name nihms86296t5.jpg
graphic file with name nihms86296t6.jpg 15 MeCN/
MeOH
(1:1)
graphic file with name nihms86296t7.jpg
5a graphic file with name nihms86296t8.jpg MeCN/
MeOH
(1:1)
graphic file with name nihms86296t9.jpg
5b 19 MeCN/
MeOH
(1:1)
graphic file with name nihms86296t10.jpg
5a graphic file with name nihms86296t11.jpg MeCN/
Tris buffer pH 8.0 (1:1)
graphic file with name nihms86296t12.jpg
graphic file with name nihms86296t13.jpg 22 MeCN/
Tris buffer pH 8.0 (1:1)
graphic file with name nihms86296t14.jpg