Skip to main content
. Author manuscript; available in PMC: 2010 Sep 9.
Published in final edited form as: J Am Chem Soc. 2009 Sep 9;131(35):12576–12578. doi: 10.1021/ja9058926

Table 2.

Radical Denitration.

graphic file with name nihms139601f6.jpg
entry 6,7 n diene yield (%)a 6:7b
1 a 1 R1=R2=CH3 67 8:1
2 b 1 R1=H, R2=CH3 53 8:1
3 c 1 R1=R2=(CH2)4 81 12:1c
4d d 1 R1=R2=Ph 83 7:1
5 e 0 R1=R2=CH3 61 1.3:1
6 f 0 R1=H, R2=CH3 35d 1.9:1
(a)

Isolated yield.

(b)

Determined by 1H-NMR.

(c)

Determined by GC.

(d)

The compound is volatile.