Table 2. Triisopropylsilanol-Catalyzed Dehydrohalogenation.
 | |
|---|---|
| solvent | distilled yield (%) |
| DMF | 77 |
| DMPU | 68 |
| xylene | 60 |
| diglyme | 50 |
| THF | a |
| DBU | 30 |
a
Product could not be separated from solvent.
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