Table 1.

Polymerization of NAS at various [M]/[CTA] ratios^a

Run No	[M]/[CTA]	[CTA]/[Initiator]	Polymerization time (h)	Conversionb(mol %)	DP theoreticalc	ASEC resultsd
						Mn (kDa)	Mw (kDa)	PD	DPe
1	100	10	1.5	77	77	5.97	6.27	1.05	84
2	200	10	2.0	60	120	8.96	9.85	1.10	126
3	300	5	2.5	48	144	1.12	1.28	1.14	158
4	400	5	3.5	48	192	1.45	1.62	1.12	204

^aPolymerization conditions: NAS (1.34 g) in DMF (4 mL, 2M solution), Temp = 70 °C

^bNAS conversion determined by ¹H NMR

^cDetermined based on conversion

^dDetermined by ASEC after ammonolysis

^eCalculated based on M_n