Table 1. Data-collection and refinement statistics.
Values in parentheses are for the highest resolution shell.
| Data statistics | |
| Space group | I23 |
| Resolution (Å) | 1.85 |
| Unit-cell parameters (Å, °) | a = b = c = 112.24, α = β = γ = 90 |
| VM (Å3 Da−1) | 2.1 |
| Solvent content (%) | 40.4 |
| Resolution range (Å) | 30.0–1.85 (1.92–1.85) |
| Measured reflections | 81063 |
| Unique reflections | 20162 (2004) |
| Rmerge† (%) | 6.7 (29.2) |
| Completeness (%) | 99.8 (99.5) |
| Average I/σ(I) | 19.5 (4.4) |
| Redundancy | 4.0 (3.9) |
| Refinement statistics | |
| Resolution (Å) | 20.0–1.85 |
| Rwork (%) | 16.4 |
| Rfree (%) | 18.4 |
| Protein atoms | 1950 |
| Water molecules | 208 |
| Phosphate ion | 1 |
| R.m.s.d. bond lengths (Å) | 0.005 |
| R.m.s.d. bond angles (°) | 1.30 |
| Estimated coordinate error (Å) | 0.16 |
| Overall B factor (Å2) | 18.90 |
| Ramachandran plot (%) | |
| Most favoured | 94.7 |
| Allowed | 5.3 |
| PDB code | 3hpd |
†
R
merge = 
, where I(hkl) is the intensity of reflection hkl, 
is the sum over all reflections and 
is the sum over i measurements of reflection h.