Table 1. Crystal and diffraction parameters for ZHE1.
X-ray source | Photon Factory AR-NW12A and BL-5A |
Wavelength (Å) | 1.000 |
Space group | P212121 |
Unit-cell parameters (Å) | a = 32.9, b = 62.5, c = 87.4 |
Resolution range (Å) | 50.0–1.14 (1.18–1.14) |
Observed reflections | 467403 |
Unique reflections | 66154 |
Data completeness (%) | 99.1 (93.9) |
Redundancy | 7.1 (5.4) |
Rmerge† | 0.058 (0.363) |
〈I/σ(I)〉 | 24.7 (4.0) |
R merge = , where I i(hkl) is the intensity of reflection hkl and 〈I(hkl)〉 is the mean intensity of reflection hkl.