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. Author manuscript; available in PMC: 2009 Nov 3.
Published in final edited form as: J Phys Chem B. 2008 Dec 25;112(51):16975–16981. doi: 10.1021/jp808012g

Figure 2.

Figure 2

Spectra from top to bottom: (A) LRAP-K54(13C′) hydrated frozen, (B) LRAP-K54(13C′) hydrated room temperature, (C) LRAP-V58(13C′) hydrated frozen, and (D) LRAP-V58(13C′) hydrated room temperature. The arrow indicates the backbone carbonyl isotropic resonance, and the asterisks indicate the spinning side bands. The loss in CP intensity (evidenced by the decrease in signal-to-noise) and the change in the spinning sideband pattern for LRAP-K54(13C′) and LRAP-V58(13C′) in the presence of water all indicate mobility on the NMR time scale (10−3–10−5 sec).