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. 2009 Oct 15;131(44):16096–16107. doi: 10.1021/ja902052v

Table 1. NOEs Observed between the AFB-α-FAPY Adduct and DNA Protonsa.

AFB-α-FAPY 10-mer ds duplex tetramer
H2α C16 H1′, C16 H3′, C16 H2′′, C16 H4′, C16 H5, C16 H6, A17 H8  
H2β A17 H8  
H3α A17 H3′  
H3β A17 H8  
H5 A17 H2, T4 H6, T4 H4′ T4 H2′, T4 H2′′
H6a T4 CH3, T4 H6, X5 H8  
H8 X5 CHO X3 CHO
H9a T4 CH3, T4 H6, T4 H1′, X5 H8  
H9    
-OCH3 A17 H2, T4 H1′, T4 H2′, T4 H2′′, T4 H5′, T4 H3, X5 H3 T4 H1′
a

NOEs involving adenine H2 protons were not included in structural refinement due to the long T1 relaxation times associated with these protons.