Table 1. Data-collection statistics.
Values in parentheses are the highest resolution shell.
| Gd-SAD | Native | |
|---|---|---|
| Beamline | ID14-4, ESRF | ID14-4, ESRF |
| Space group | P43212 | P43212 |
| Unit-cell parameters (Å) | ||
| a | 60.9 | 61.3 |
| b | 60.9 | 61.3 |
| c | 166.5 | 165.7 |
| Resolution (Å) | 50–2.1 (2.21–2.10) | 50–2.0 (2.11–2.00) |
| Wavelength (Å) | 0.98 | 0.98 |
| No. of unique reflections | 18230 (2068) | 22215 (3200) |
| Multiplicity | 15.4 (7.3) | 4.4 (4.6) |
| Completeness (%) | 95.3 (77.3) | 99.7 (100) |
| 〈I/σ(I)〉 | 24.4 (5.5) | 11 (3.6) |
| Rmerge† (%) | 7.6 (24.9) | 8.0 (39.1) |
| Ranom‡ (%) | 2.5 (10.6) | |
| FOM§ | 0.31 | |
| FOM (after DM) | 0.79 | |
| Phasing power | 1.20 | |
| RCullis | 0.78 |
R
merge =
.
R
anom =
.
Figure of merit.