Table 1. Data-collection statistics.
Values in parentheses are for the last resolution shell.
| Synchrotron beamline | PAL 6C1 |
| Wavelength (Å) | 0.96418 |
| Unit-cell parameters | |
| a = b (Å) | 69.5 |
| c (Å) | 154.4 |
| α = β (°) | 90 |
| γ (°) | 120 |
| Space group | P3221 |
| Resolution (Å) | 50.00–1.90 (1.97–1.90) |
| Total No. of reflections | 32228 |
| No. of unique observations | 2036 |
| Redundancy | 10.5 (10.2) |
| Completeness (%) | 92.2 (59.3) |
| Molecules per ASU | 2 |
| VM (Å3 Da−1) | 3.2 |
| Solvent content (%) | 61.7 |
| Rmerge† (%) | 0.051 (0.477) |
| I/σ(I) | 63.1 (5.6) |
R
merge =
, where I
i(hkl) is the intensity of the ith observation of reflection hkl and 〈I(hkl)〉 is the average intensity of reflection hkl.