Table 1. Crystallographic data-collection and refinement statistics.
Values in parentheses are for the highest resolution shell.
| Data-collection statistics | |
| Space group | P42212 |
| Unit-cell parameters (Å) | a = b = 99.14, c = 229.06 |
| Resolution (Å) | 50.0–4.7 (4.95–4.7) |
| Rmerge† (%) | 8.3 (40.7) |
| Completeness (%) | 91.0 (92.7) |
| I/σ(I) | 10.4 (2.99) |
| No. of reflections | 21804 (3122) |
| No. of unique reflections | 5856 (817) |
| Molecular-replacement statistics | |
| Resolution (Å) | 15.0–4.7 |
| Two-body rigid-body refinement | |
| Correlation coefficient (%) | 68.2 |
| R factor‡ (%) | 52.3 |
| Seven-body rigid-body refinement | |
| Correlation coefficient (%) | 69.8 |
| R factor‡ (%) | 50.9 |
R
merge =
.
R =
. The R factor is calculated on all reflections.