Table 2. Crystallographic data-collection statistics for the selenomethionine-labelled crystal.
Values in parentheses are for the highest resolution shell.
| Peak | Edge | Remote | |
|---|---|---|---|
| Wavelength (Å) | 0.97831 | 0.97928 | 0.96405 |
| Beamline | PF BL-17A | ||
| Space group | C2 | ||
| Unit-cell parameters | |||
| a (Å) | 245.8 | ||
| b (Å) | 148.7 | ||
| c (Å) | 119.9 | ||
| β (°) | 112.9 | ||
| Resolution (Å) | 50.00–2.40 (2.49–2.40) | 50.00–2.40 (2.49–2.40) | 50.00–2.50 (2.59–2.50) |
| Measured reflections | 1150410 | 1142105 | 1021559 |
| Unique reflections | 154893 | 154939 | 137340 |
| Completeness (%) | 99.7 (97.4) | 99.7 (97.1) | 99.8 (97.9) |
| Redundancy | 7.5 (5.8) | 7.4 (5.6) | 7.5 (5.9) |
| Mean I/σ(I) | 20.2 (3.2) | 19.9 (3.0) | 18.8 (3.1) |
| Rmerge† (%) | 10.3 (27.6) | 11.7 (29.1) | 11.2 (28.5) |
†
R
merge = 
, where Ii(hkl) is the intensity of the ith measurement of reflection hkl and 〈I(hkl)〉 is the mean value of Ii(hkl) for all i measurements.