TABLE 1.
Summary of crystallographic data
| Wild type SmTGR | |
|---|---|
| Data collection | |
| Space group | C2 |
| Cell dimensions | |
| a, b, c (Å) | 147.51, 102.16, 60.57 |
| α, β, γ (°) | 90.00, 114.15, 90.00 |
| Resolution (Å) | 40.0-2.55 (2.59-2.55)a |
| Rmerge | 0.12 (0.48) |
| I/σI | 14.7 (2.4) |
| Completeness (%) | 99.7% (99.9%) |
| Redundancy | 5.2 (5.2) |
| Refinement | |
| Resolution (Å) | 40.0-2.55 |
| No. reflections | 25362 |
| Rwork/Rfree | 0.231/0.256 |
| No. of atoms (1 subunit/au) | 4745 |
| Protein | 4540 |
| Ligand/ion | 104 |
| Water | 101 |
| B-factors (overall) | 35.42 |
| Root mean square deviations | |
| Bond lengths (Å) | 0.006 |
| Bond angles (°) | 0.91 |
| Ramachandran plot | |
| Most preferred | 90.4% |
| Allowed | 9.2% |
| Generously allowed | 0.4% |
a
Highest resolution shell is shown in parentheses.