Table I.
Data collection and refinement statistics
Velaglucerase alfa | |
---|---|
Data collection | |
Space group | C2221 |
Cell dimensions | |
a, b, c (Å) | 109.37, 285.55, 91.69 |
abg (°) | 90.00, 90.00, 90.00 |
Resolution (Å) | 19.9–2.7 (2.75–2.70)a |
Rsym(%) | 15.7 (51.0) |
I/s<I> | 14.4 (4.6) |
Completeness (%) | 100 (100) |
Redundancy | 7.5 (7.6) |
Refinement | |
Resolution (Å) | 19.9–2.7 |
Number of reflections | 39,776 |
Rwork/Rfree | 17.3/23.4 |
Rms deviations | |
Bond lengths (Å) | 0.012 |
Bond angles (°) | 1.486 |
Number of refined atoms | |
Protein | 7871 |
Carbohydrates | 70 |
Ions | 90 |
Solvent | 326 |
Ramachandran outliers (%) | 0.4 |
aThe highest resolution shell is shown in parentheses.