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. Author manuscript; available in PMC: 2010 Dec 1.
Published in final edited form as: Dent Mater. 2009 Aug 25;25(12):1569–1575. doi: 10.1016/j.dental.2009.07.010

Fig. 3.

Fig. 3

Representative tan delta versus temperature curves of control (C0, C8, C16) and experimental (E0, E8, E16) adhesive polymers with 0%, 8% and 16% water contents. The polymerized samples were stored in the vacuum oven under drying agent at 37 °C for 1 week after curing. DMA (TA Instruments, Q800) with a three-point bending clamp was conducted over a temperature range of 0 ~ 200 °C with a ramping rate of 3 °C/min at a frequency of 1 Hz. n = 5 +/ S.D.