Table 2.

Data Reduction Statistics for WT HbI Time-resolved Laue Data

Statistics for representative WT HbI crystals for Series 1 and Series 2 (20 images per dark/light data set for each crystal; 9° angular increment)
Series	Crystal	Time delay	X-ray exposure time	R(F2) (%)	R(|F|) (%)	Completeness (%)
						Overall 100-1.6 Å	Last Shell 1.67-1.6 Å
1	1 of 3	dark	100ps ×177	5.4	3.1	62.7	22.5
1	1 of 3	5ns	100ps × 75	5.9	3.5	54.6	14.6
1	1 of 3	25ns	100ps × 75	5.9	3.5	54.3	14.2
1	1 of 3	75ns	100ps × 75	6.1	3.6	53.1	13.9
1	1 of 3	200ns	100ps × 75	6.5	3.7	51.8	13.4
2	1 of 3	dark	500ns × 20	4.1	2.5	65.1	26.1
2	1 of 3	500ns	500ns × 15	5.0	3.1	57.4	19.7
2	1 of 3	1μs	500ns × 15	4.7	2.9	59.5	20.5
2	1 of 3	2μs	500ns × 15	4.5	2.7	60.1	21.4
2	1 of 3	4μs	500ns × 15	4.4	2.7	60.2	21.1
2	1 of 3	6μs	500ns × 15	4.6	2.8	60.1	21.2
2	1 of 3	30μs	500ns × 15	4.6	2.8	60.1	21.2
Completeness of ΔF(t) WT HbI data sets (ΔF(t) merged across 3 crystals)
Resolution range (Å)	5ns	25ns	75ns	200ns	500ns	1μs	2μs	4μs	6μs	30μs
100 – 1.60	70.5	69.1	68.6	66.1	71.4	72.9	73.2	72.4	72.6	72.5
100 – 3.20	85.0	79.8	80.9	75.3	75.2	77.6	78.7	73.4	74.6	73.3
3.20 – 2.54	90.4	89.3	89.7	88.1	89.9	90.4	90.7	90.1	89.9	90.6
2.54 – 2.22	88.2	87.2	86.7	85.8	89.2	90.1	89.7	89.8	90.1	89.6
2.22 – 2.02	85.7	85.9	84.8	83.9	87.2	88.5	88.4	88.5	88.8	88.6
2.02 – 1.87	73.7	73.8	73.0	70.5	76.4	78.5	78.4	78.5	78.2	78.6
1.87 – 1.76	62.2	60.9	59.5	57.2	66.1	67.1	67.7	67.6	67.9	67.6
1.76 – 1.67	49.4	48.8	47.5	43.6	53.9	55.9	56.4	56.6	56.2	57.2
1.67 – 1.60	29.6	27.4	26.5	24.5	33.6	35.1	35.4	35.8	35.2	34.9