Table 1. 1H chemical shifts of the COOH-terminal residues of dogfish αB-crystallin in 10 mM phosphate buffer, pH 6.5, at 25 °C.
Residue | NH | Hα | Hβ | Others |
---|---|---|---|---|
V162 |
8.14 |
4.44 |
1.86 |
γCH3, 0.98 |
P163 |
|
4.40 |
1.88 |
|
I164 |
8.00 |
4.36 |
2.09 |
γCH2, 1.22; γCH3, 0.96 |
S165 |
8.39 |
4.69 |
4.06, 4.03 |
|
R166 |
8.32 |
4.38 |
1.85, 1.97 |
γCH2, 1.75; δCH2, 3.22 |
D167 |
8.26 |
4.80 |
2.65, 2.75 |
|
E168 |
8.38 |
4.30 |
2.01, 2.14 |
γCH2, 2.41 |
K169 |
8.34 |
4.40 |
1.64, 1.78 |
|
P170 |
|
4.45 |
2.28 |
|
A171 |
8.30 |
4.37 |
1.44 |
|
V172 |
8.14 |
4.20 |
1.86 |
γCH3, 0.90 |
A173 |
8.31 |
4.32 |
1.39 |
|
G174 |
8.12 |
4.18 |
||
P175 |
|
4.46 |
1.92 |
γCH2.20, 1.98; δCH3.64, 3.66 |
Q176 |
8.26 |
4.36 |
2.02, 2.14 |
γCH2, 2.38 |
Q177 |
8.42 |
4.35 |
1.99, 2.13 |
γCH2 2.41 |
K178 | 7.94 | 4.18 | 1.73, 1.85 | γCH2 1.41, εCH2 2.69 |