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. 2009 Dec 21;15(47):5992–5999. doi: 10.3748/wjg.15.5992

Table 1.

Parameters of the 6 major DCQD components in rat plasma QC samples (%, n = 6)

Spiked amount (ng/mL) Intra-day
Inter-day
Extract
RSD Ac RSD Ac Recovery RSD
Rhein 39.1 3.76 104.60 3.53 107.94 104.60 3.76
156 5.55 100.32 5.52 106.87 100.32 5.55
625 5.31 101.07 5.56 105.36 101.07 5.31
3750 4.24 101.24 6.23 98.37 101.24 4.24
Chrysophanol 6.1 2.37 99.4 4.46 98.67 99.39 2.36
24.4 4.38 104.17 4.88 101.14 104.17 4.37
97.7 1.64 96.66 3.33 98.09 96.66 1.64
586 3.78 103.98 4.44 101.13 103.98 3.78
Rheochrysidin 39.1 5.69 97.70 5.72 100.78 97.69 5.68
156 3.33 99.89 4.13 101.14 99.89 3.33
625 3.22 105.92 3.73 104.37 105.92 3.22
3750 4.75 103.07 4.84 103.49 103.07 4.75
Magnolol 6.1 5.51 102.13 5.07 106.33 102.13 5.51
24.4 2.39 104.78 5.79 99.86 104.78 2.39
97.7 5.51 107.81 4.92 106.23 102.47 5.51
586 3.77 105.97 5.33 105.29 105.97 3.77
Hesperidin 6.1 4.12 95.96 4.82 98.49 95.96 4.12
24.4 5.83 99.52 5.10 100.29 99.52 5.83
97.7 4.21 100.14 3.95 99.72 100.16 4.21
586 2.77 97.13 4.91 98.52 97.13 2.76
Naringin 6.1 2.66 95.66 4.26 99.29 95.67 2.657
24.4 2.82 102.46 3.95 103.37 102.45 2.82
97.7 3.81 100.78 3.96 100.66 100.78 3.81
586 5.24 98.27 5.59 99.32 98.27 5.24

DCQD: Da-Cheng-Qi Decoction; QC: Quality control.