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. 2010 Jan 5;5(1):e8565. doi: 10.1371/journal.pone.0008565

Table 2. T Dispersion Analysis of Crosslinked BSA and Tissues.

γB1 Values (kHz) Model Curve Fit (% Standard Error of the Estimate) Relaxation-Time Power Law (Eq. [1]) Parameters of Fit
Sample Groups Samples Number of values Minimum Maximum Relaxation-Time Power Law Eq. [1] Relaxation-Rate Power Law Eq. [2] BPP Model Eq. [3] “a” (ms) “b” (10−6×sec1+C) “c” (exponent)
BSA (Fraction V) in H2O (2T) 10% BSA, 80mM GA 13 0.97 60.0 2.4 6.8 2.9 138 764 0.515
10% BSA, 100mM GA 13 1.01 59.2 2.1 5.3 5.0 93.8 2247 0.425
20% BSA, 200mM GA 22 0.14 33.1 2.3 12 3.3 45.7 31.1 0.731
BSA (Monomers) in H2O (2T) 10% BSA, 60mM GA 13 1.50 33.1 0.4 9.7 0.9 293 3.10 0.993
10% BSA, 80mM GA 13 1.50 33.1 0.8 17 1.5 187 21.7 0.833
10% BSA, 100mM GA 13 1.50 33.1 0.9 4.0 1.9 133 298 0.596
BSA (Fraction V) in H2O (4.7T) 10% BSA, 60mM GA 23 1.05 154 1.2 10 7.3 155 334 0.591
10% BSA, 80mM GA 19 1.50 100 2.0 4.7 4.5 81.8 2464 0.411
10% BSA, 200mM GA 23 1.00 154 3.0 9.4 9.5 64.2 785 0.501
10% BSA (Fraction V), 60mM GA (2T) undialyzed 23 0.10 33.1 1.2 8.2 1.9 156 42.7 0.757
dialyzed in excess DMSO 23 0.10 33.1 2.7 18 1.8 53.2 3.98 0.964
dialyzed in H2O 15 0.79 22.8 1.4 4.8 2.8 91.9 466 0.577
4.7T rabbit myocardial tissue 19 0.59 47.6 2.0 7.2 8.4 74.5 398 0.569
2T rat myocardial tissue 22 0.10 28.5 1.2 12 3.4 68.4 26.9 0.786
Cartilage (2T) in saline 23 0.21 46.0 1.7 6.0 2.9 87.4 509 0.484
in DMSO 24 0.21 56.0 3.6 17 3.9 9.06 5.87 0.756
in phosphate buffer pH 9.2 21 0.20 33.1 3.9 17 4.2 26.9 25.8 0.769
in phosphate buffer pH 7.0 23 0.10 33.1 3.3 13 4.1 51.0 224 0.591
in phosphate buffer pH 4.35 23 0.10 33.1 4.1 16 4.7 39.6 133 0.635

BSA = Bovine serum albumin, GA = Glutaraldehyde, DMSO = Dimethyl sulfoxide.