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Cyclic voltammograms of a 0.2 mM solution of complex 1 containing 0.1 M tetrabutylammonium hexafluorophosphate in A) THF (left) and B) DMF (right) at a scan rate of 50 mV/s. The measurements were carried out with a Pt electrode and referenced to the Fc/Fc+ redox couple. Differential pulse voltammograms of 1 and 2 are shown in the Supporting Information (Figure S8 and S9, respectively).
