Table 1.
Characterization of surface functional groups present on MWCNT using a Knudsen flow reactor.
Gas [gas-phase probe molecules] | N(CH3)3 [acidic sites] | HCl [basic sites] | CF3COOH [basic sites] | NH2OH [carbonyl functions] | O3 [oxidizable sites] | NO2 [oxidizable sites] |
---|---|---|---|---|---|---|
no/mga | 3.0.1015 | 8.1.1016 | 2.4.1016 | 2.4.1017 | 3.9.1018 | 1.2.1016 |
no/cm2b | 1.4.1012 | 3.7.1013 | 1.1.1013 | 1.1.1014 | 1.8.1015 | 5.3.1012 |
MLc | 0.28% | 7.4% | 2.2% | 22% | 360% | 1.1% |
Results are expressed as indicated in footnotes a, b and c and using a BET surface of 219.2 m2/g.
number of probe molecules taken up per mg of deposited nanoparticles
number of probe molecules taken up per square cm of MWCNT (no/cm2)
number or fraction of formal monolayer (ML) of reacted probe gas using an average of 5x1014 molecules cm-2 as one formal ML.