Table 1. Data-collection and refinement summary.
Values in parentheses are for the highest resolution shell.
| Data collection | |
| Space group | P4212 |
| Unit-cell parameters () | a = b = 138.7, c = 186.8 |
| No. of molecules in the ASU | 4 |
| Resolution () | 2.8 |
| R merge | 9.3 (36) |
| I/(I) | 17.32 (3.56) |
| Completeness | 99.6 (98.2) |
| Refinement | |
| Refinement program | REFMAC5 |
| Reflections in the working set | 41393 |
| Reflections in the test set | 2179 |
| R factor (%) | 20.8 |
| R free (%) | 25.6 |
| No. of atoms modelled | 10565 |
| No. of waters | 33 |
| Average B factor (2) | 38.1 |
| Average B factor, solvent (2) | 25 |
| R.m.s.d. from ideal | |
| Bond lengths () | 0.009 |
| Angles () | 1.18 |
| Ramachandran plot | |
| Most favoured (%) | 91.6 |
| Additionally allowed (%) | 8.1 |
| Generously allowed (%) | 0.3 |
| Disallowed (%) | 0 |