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DAAA of Allyl Enol Carbonates of Various Acyclic Alkyl, Alkenyl and Alkynyl Ketones
 | |||||
|---|---|---|---|---|---|
| entry | Substrate (Z/E) |
product | time | yield | ee |
| 1 |
2 (>98/2) |
 |
5 h | 94% | 88% |
| 2 |
101 (25/1) |
 |
0.3h | 93% | 91% |
| 3 |
16 (>98/2) |
 |
16 h | 99%a | 46% |
| 4 |
16 (1/23) |
103 | 16 h | 99%a | 94% |
| 5 |
17 (1/18) |
 |
16 h | 99%a | 88% |
| 6 |
18 (1/14) |
 |
2 h | 91% | 81% |
Conversion based on GC analysis.
