TABLE 1.
Data collection and refinement statistics
| Parameter | Value for Nativea |
|---|---|
| Data collection | |
| Space group | I23 |
| Cell dimensions | |
| a = b = c (Å) | 303.431 |
| Resolution (Å) | 30-3.35 (3.47-3.35) |
| Rsym | 0.080 (0.379) |
| <I>/<σI> | 14.6 (3.3) |
| Completeness (%) | 99.7 (98.3) |
| Redundancy | 4.5 (3.2) |
| Refinement | |
| Resolution (Å) | 30-3.35 |
| No. of reflections | 65,456 |
| Rwork/Rfree | 0.2171/0.2334 |
| No. of atoms | |
| Protein | 16,056 |
| Ions | 6 |
| Water | 10 |
| Avg B factor (Å2) | |
| Protein | 100.0 |
| Ions | |
| Water | 37.8 |
| RMSD | |
| Bond lengths (Å) | 0.005 |
| Bond angles (°) | 0.918 |
| NCS pairs AB, AC, AD, AE (Å) | 0.014, 0.016, 0.013, 0.021 |
a
Values corresponding to the highest resolution shell are shown in parentheses.