Table 1. Diffraction data and refinement statistics for hDAO form I.
Values in parentheses are for the highest resolution shell.
| Space group | C2221 |
| Unit-cell parameters (Å) | a = 94.8, b = 97.0, c = 178.1 |
| X-ray source | AUS 3BM1/rotating anode |
| Wavelength (Å) | 0.95663/1.5418 |
| Detector | ADSC Quantum 210r/MAR 345 |
| Resolution range (Å) | 178.1–2.1 (2.21–2.10) |
| Observed reflections | 332912 |
| Unique reflections | 45200 |
| Completeness (%) | 95.2 (96.2) |
| Multiplicity | 7.4 (3.0) |
| 〈I/σ(I)〉 | 15.7 (2.5) |
| Rmerge† | 0.11 (0.3) |
| Rp.i.m.‡ | 0.03 (0.19) |
| Reflections in working set | 42911 |
| Reflections in test set | 2288 |
| Protomers per ASU | 1 |
| Total atoms (non-H) | 5983 |
| Protein atoms | 5605 |
| Metal atoms | 3 |
| Water atoms | 299 |
| Atoms in alternate conformers | 34 |
| Other atoms | 76 |
| Rcryst | 0.236 (0.321) |
| Rfree | 0.290 (0.367) |
| R.m.s.d. bond lengths (Å) | 0.009 |
| R.m.s.d. bond angles (°) | 1.2 |
| 〈B〉 (Å2) | 26.0 |
| Cruickshank’s DPI§ (Å) | 0.3 |
| PDB code | 3k5t |
