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. 2009 Nov 20;38(3):1048–1056. doi: 10.1093/nar/gkp1022

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© The Author(s) 2009. Published by Oxford University Press.

This is an Open Access article distributed under the terms of the Creative Commons Attribution Non-Commercial License (http://creativecommons.org/licenses/by-nc/2.5/uk/) which permits unrestricted non-commercial use, distribution, and reproduction in any medium, provided the original work is properly cited.

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Scheme 3. — Synthesis of 6-Phenylpyrrolocytidine phosphoramidite (7). a. I₂, AgSO₄, MeOH. b. DMT-Cl, py. c. phenylacetylene, DMF, Pd(PPh₃)₄, CuI, NEt₃. d. AgNO₃, acetone. e. NH₄OH, MeOH, 55°C. f. TBDMS-Cl, imidazole, DMF. g. (iPr)₂NP(Cl)O(CH₂)₂CN, THF, NiPr₂Et.