Table 1.
Data Collection and Refinement Statistics
| TopBP1 BRCT6 | |
|---|---|
| Data Collection | |
| Space group | P212121 |
| Unit-cell parameters (Å) | a = 35.77, b = 51.82, c = 62.09 |
| Resolution range (Å) | 50–1.34 (1.39–1.34) |
| No. of reflections | 173,010 |
| Unique reflections | 26,433 (2396) |
| Rsyma (%) | 4.3 (32.6) |
| I/σ(I) | 30.2 (2.1) |
| Completeness (%) | 99.0 (91.6) |
| Redundancy | 6.5 (3.3) |
| Refinement | |
| Resolution (Å) | 39.78–1.34 |
| No. of reflections | 25,049 (1644) |
| Rwork/Rfree (%)b | 15.8/17.3 |
| No. of atoms | |
| Overall | 971 |
| Protein | 818 |
| Waters | 153 |
| Average B factor (Å2) | |
| Overall | 12.11 |
| Protein | 9.97 |
| Waters | 23.57 |
| R.m.s. deviations | |
| Bonds (Å) | 0.009 |
| Angles (°) | 1.208 |
| Ramachandran | |
| Most favored (%) | 90.5 |
| Additionally allowed (%) | 9.5 |
| Generously allowed (%) | 0 |
a
Rsym = S|I−〈I〉|2/S|I2|
b
R = S||Fo|−|Fc||/S|Fo|, Rfree was calculated from 5% of the data excluded from refinement.