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. Author manuscript; available in PMC: 2011 Feb 10.
Published in final edited form as: J Am Chem Soc. 2010 Feb 10;132(5):1482. doi: 10.1021/ja910154f

Table 2.

Radical haloalkylation: haloalkylating agent scope.

graphic file with name nihms169677t10.jpg
entry product yield
dra 		entry product yield
dra
1 graphic file with name nihms169677t11.jpg 64%
>98:2		 4 graphic file with name nihms169677t12.jpg 75%
1.3:1b
2 graphic file with name nihms169677t13.jpg 83%
>98:2		 5 graphic file with name nihms169677t14.jpg 71%
1.6:1b
3 graphic file with name nihms169677t15.jpg 71%
>98:2		 6 graphic file with name nihms169677t16.jpg 76%
>98:2
a

All reported yields are of isolated products, dr was determined by 500 MHz 1H NMR.

b

at the indicated stereocenter