Table I.
Data Collection and Refinement Statistics
| Data collection at 1.9995 Å | |
| Resolution (Å) (last shell) | 28–2.3 (2.44–2.3) |
| Observed reflections | 1.130368 |
| Unique reflections | 8736 |
| Completeness | 97.3 (97.3) |
| Redundancy | 31.1 |
| Rsyma | 8.6 (33.9) |
| Unit cell dimensions (Å, °) | |
| a/b and c | 80.23/50.71 and 54.19 |
| β | 117.094 |
| Refinement statistics | |
| R-factorb (%) | 22.1 (42.7) |
| Rfree (%) | 27.6 (45.8) |
| Bond lengthc (Å) | 0.006 |
| Bond anglesc (°) | 1.3 |
| Ramachandran plotd | 87.5/12.5/0/0 |
a
Rsym = 100* Σ|I − 〈I〉|/ΣI. Values for the final resolution shells are in parenthesis.
b
Rfactor = 100* Σ||Fobs| − |Fcalc||/Σ|Fobs|.
c
Root mean square error.
d
Percentage of residues in most favored/additionally allowed/generously allowed, and disallowed regions.