TABLE 1.
Crystal data
| Crystals | ||
| Sgf11 fragment | 7–33 | 1–33 |
| Space group | P61 | P61 |
| Unit cell dimensions (Å) | ||
| a | 75.15 | 68.67 |
| b | 75.15 | 68.67 |
| c | 197.37 | 232.86 |
| Data collection | ||
| Wavelength (Å) | 1.54059 | 1.0719 |
| Resolution range (Å)a | 25–2.1 (2.21–2.1) | 59.4–2.7 (2.85–2.7) |
| Total observationsa | 503,521 (37,147) | 382,872 (56,409) |
| Unique observationsa | 36,176 (5,136) | 17,082 (2,485) |
| Completeness (%)a | 98.3 (95.3) | 100 (100) |
| Multiplicity | 13.9 (7.2) | 22.4 (22.6) |
| Rpim (%)a | 1.5 (29.2) | 2.4 (29.7) |
| Rmerge (%)a | 5.9 (75.7) | 11.2 (138.6) |
| Mean I/σ(I)a | 26.2 (2.4) | 18.1 (2.7) |
| Refinement | ||
| Rcryst/Rfree (%) | 19.0/23.7 | 21.3/25.3 |
| Bond length r.m.s.d. (Å)b | 0.002 | 0.002 |
| Bond angle r.m.s.d. | 0.6° | 0.62° |
| MolProbity score/percentile | 1.41/99 | 2.10/97 |
| Ramachandran plot (%) | ||
| Favoured | 99.5 | 98.4 |
| Allowed | 0.5 | 1.6 |
| Forbidden | 0 | 0 |
| PDB accession codec | 3KIK | 3KJL |
a Parentheses refer to final resolution shell.
b r.m.s.d., root mean square deviation.
c PDB, Protein Data Bank.